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Beilstein J. Org. Chem. 2018, 14, 3070–3075, doi:10.3762/bjoc.14.285
Graphical Abstract
Figure 1: Some bioactive molecules containing hydroxamate functionality.
Scheme 1: Cross metathesis between a class-I alkene and N-benzyloxyacryl amide.
Beilstein J. Org. Chem. 2017, 13, 2153–2156, doi:10.3762/bjoc.13.214
Figure 1: Biologically active naturally occurring cyclic tetrapeptide HDAC inhibitors.
Scheme 1: Reagents and conditions: (i) Triethyl phosphonoacetate, n-Bu4N+I−, aq K2CO3, rt, 18 h, 86%; (ii) H2...
Scheme 2: Reagents and conditions: (i) Grubbs’ catalyst 12 (2.5 mol %), DCM, reflux, 2 h, 14a, 83%; 14b, 90%; ...
Beilstein J. Org. Chem. 2015, 11, 2487–2492, doi:10.3762/bjoc.11.270
Figure 1: Structure of FR-225497 (4) and related cyclic tetrapeptides.
Figure 2: Synthetic planning for the design of analogues of 4.
Scheme 1: Preparation of the macrocyclic template 13.
Scheme 2: Synthesis of nor-FR225497 (15).
Scheme 3: Synthesis of oxygenated ethyl vinyl ketones.
Scheme 4: Synthesis of analogues of FR-225497.